Published September Origi- nally approved in Last previous edition approved in as 3. E – 89a (). Annual Book of ASTM Standards. Buy ASTM E TEST METHODS FOR CHEMICAL ANALYSIS OF COPPER ALLOYS from SAI Global. These test methods for the chemical analysis of metals and alloys are primarily intended as referee methods to test such materials for.
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The addition of 1 g of benzoic acid per litre will prevent bacterial growth. Stir the mixture vigorously and allow to cool to room temperature while stirring occasionally.
Draw off the organic phase and discard, being careful to avoid any losses of the aqueous solution in this operation and the subsequent phase separations. Summary of Test Method Users are encouraged to use these or similar reference materials to verify that the method is performing accurately in their laboratories.
Users are encouraged to employ suitable reference materials, if available to verify the accuracy of the method in their laboratories. The extraction procedure also affords a separation of the zinc from cadmium. Users are encouraged to use this or similar reference materials to verify that the method is performing accurately in their laboratories. Silicon bronze NIST a 0. Users are encouraged to employ suitable reference materials, if available, to verify the accuracy of the method in their laboratories.
asrm No other units of measurement are included in this standard. The variability of the readings of the highest calibration solution and of the reference solution must be less than 3.
Standard Test Methods for Chemical Analysis of Copper Alloys
A superscript epsilon e indicates an editorial change since the last revision or reapproval. Work in a well-ventilated hood. Avoid inhalation of fumes and exposure of skin to the chemical and its solutions. The precipitate is dissolved in hydrochloric acid and the tin is reduced with iron and nickel and titrated with a standard potassium iodate solution in an inert atmosphere.
Platinum gauze anodes should be made of the same material and of the same general design as platinum gauze cathodes.
ASTM E – 08 Standard Test Methods for Chemical Analysis of Copper Alloys
Please login to your authorized staff account to use this feature. Cast bronze NIST 52c, 0. Silicon bronze NIST a, 1. It is expected that work will be performed in a properly equipped laboratory. The absorption by the sample solution of the silver resonance line energy at AAB 1 2 We have no amendments or corrections for this standard. After the blue color due to copper has disappeared, wash the cover glasses, electrodes, and the sides of the beaker, and continue the electrolysis ast deposition of the copper is complete, as indicated by failure to plate on a new surface when the level of the solution is raised.
Cover the beaker with a raised cover glass, and evaporate the solution to a volume of 2 to 3 mL. Nails, Spikes, and Staples. Calibration 1 2 0. Evaporate till nearly to dryness. Apply the sensitivity test and curve linearity test as directed in Using the test cell, take the photometric readings of the calibration solutions.
Add HF as needed to decompose high-silicon alloys. This standard is also available to be included in Standards Subscriptions. Add 10 mL of HCl and dilute e78 1 L. The cathode should be stiffened by doubling the gauze for about 3 mm at the top and the bottom of the cylinder or by reinforcing the gauze at the top and bottom with a platinum band or ring.
Iron by the 1,Phenanthroline Photometric Test Method [0. When used in analyses where both cathodic and anodic plates are to be determined, the anodes should be of wire gauze.
Asfm you sure you want to empty the cart? Quickly remove the cathode, rinse it in water, and then dip into two successive baths of ethanol or methanol.
ASTM E478 – 08(2017)
Dilute to volume, and mix. Heat to copious white fumes and boil to destroy organic matter. There were no books found for the applied search filters. Repeat at least twice with no change in parameters.
Add to the beaker the weight of copper purity, Calculate the percentage of tin as follows: Add 8 mL of the DDC solution for each 0. Do not use a solution that has stood for more than 3 months. Add 5 mL more of diethyldithiocarbamate solution to the separatory funnel and mix.
Starch is used to indicate the end point. Cover with a cover glass and allow to stand for a few minutes until the reaction has nearly ceased. E Standard Terminology Relating to Metallography. The sstm variability for the highest calibration solution should be less than 1.